SynFlup
The Synthesis Fluidic Platform “SynFluP” is dedicated to Organic Synthesis in Continuous Reactor
available to anyone through collaboration or service, or just for quick test !
Better process safety
by lowering down
reactor dimensions
even for larger scale !
COLD
-80°C
REAGENT
compatible with
most reagents
Photo
Chemistry
1 flow equipement
SAFETY
unstable reagent
explosive, CMR
MICROMIXER
4 Small micromixers
1 large scale mixer
SUSPENSION
Fine suspension
Pd/C, NaBH4
Better mixing
using specially designed micromixers, from 100µL/min to 10mL/min
Fine suspension are
tolerated
Heterogeneous catalyst
from 500mg to 30g
GREEN
Less reagents
Less energy
Kinetics
from 5 ms
to 1h
GAS/LIQUID
Hydrogen, oxygen
carbon dioxide
Temperature range :
-80°C to 250°C
Pressure range:
1 bar to 200 bar
Most reagents and solvent are compatibles :
bases, acids, hydrides, Grignards, OrganoLithium, Lewis acids, ...
Activation using non classical conditions :
photochemistry, photocatalysis
supercritiacl fluids (water, CO2, DMC)
Greener process by
lowering down energy
usage, reagent excess and
fewer by-products
HEAT
up to 250°C
Amenable to ultrafast reactions (sub second)
to slower ones
(one hour max)
SOLVENT
almost no solvent limitation
Possible addition of
gas (H2, CO2, O2)
with tube in tube
or mass flow controler
SUPER
CRITICAL
Jasco System
2 reagents / gas
Description of Equipment
Uniqsis FlowSyn
FlowSyn combines all the benefits of the FlowSyn system to deliver a compact, fully integrated, easy-to-use continuous flow reactor for single reactions. FlowSyn’s high resolution user interface quickly guides you through the process for setting up a flow chemistry reaction with two reagents. Once set up, FlowSyn automatically runs the experiment unattended, ensuring that critical parameters remain within defined limits.The system can easily be reconfigured for a variety of experiments. Carry out superheated reactions up to +150°C and small scale cooled reactions down to -78°C
Vapourtec R4-R2+ unit
This unit provides the basic entities to preform reaction test with flexible HPLC pumps with ceramic heads inerted with PTFE and capable of handling strong acids such as HNO3. The coiled reactor is made in fluoropolymers and can be heated through the system from Room Temperature to 120°C, depending on required pressure. Additionally a module for heterogeneous reactions is available with columns of various capacities (from 7mL up to 50mL) able to work under the same temperature conditions. The pressure in the system is limited by the fittings at 30bar.
Vapourtec V-3 Easy Scholar Unit
This unit provides an advanced entry in unsafe reagents handling. The peristaltic pumps have very little pulsation and are able to handle slurries, strong oxidant and reducing agents. The digital command enables a quick and handy management of pumps, valve and collection. The reaction temperature can be fixed between Room Temperature and 120°C. Reaction pressure is limited by the capacities of peristaltic pumps at 10bar.